Progress Update on SABRE Crystal Growth Project
The SABRE Crystals
Frank Calaprice
SABRE PoP
NaI(Tl)
Crystal
P
r
o
d
u
c
e
r
:
P
r
i
n
c
e
t
o
n
U
n
i
v
e
r
s
i
t
y
&
R
M
D
C
o
m
p
a
n
y
(
B
o
s
t
o
n
)
•
Starting point: Astrograde powder by Sigma Aldrich with 9 ppb
nat
K.
•
In fall 2015 RMD
grew
a 2
-
kg crystal (3.5” diameter) with:
•
9 ppb
nat
K (same as starting powder)
•
< 0.1 ppb
87
Rb
Measured by ICP-MS: F
irst
crystal
below DAMA (
[K]
~13 ppb
, [Rb]<0.35 ppb)
•
Research
since the
n
focused on
:
•
G
rowing full
-
scale
5-kg
crystal (
≈ 4” diameter
)
•
improving
procedure
s
for crystal growing to reduce background
•
P
owder drying
, crucible purity, etc.
•
Refined procedure for crystal
handling
(polishing, crystal mounting and handling
inside the enclosure in glove box
)
•
Facilities at PU: new glove box installed inside Rn-free clean room
Growth setbacks:
Impurities in crystal-grade powder- now understood (?)
RMD funded by DoE (1 M$) -> extra 50 kg of Astrograde powder 3 ppb in K
Test growth of full-scale crystal with Astrograde Powder (AP) August 2017
1st crystal
with RMD AP and crucible: Oct
3 2017 (still cooling
…
)
2nd crystal
with PU AP and crucible: Nov. 2017 (starting soon)
Glove box @ PU
Princeton SABRE Crystal Group -July 2017
Small Oven System for Crystal Growing Tests.
Small 2-inch Crystal grown in Princeton
SABRE PoP Summary
•
Setbacks in crystal growth, delay of site preparation, and delay in purchase orders, all introduced several months
of delay. We passed these problems and expect to good progress now.
•
Growth of 1st 5-kg crystal is expected to finish in early October. A second will come in November.
•
Fluid operations, blocked by laboratory management, can start under new agreement with Regional Authorities.
With completed Safety Review, cleaning with fluids and scintillator operations should start soon.
•
Most of the major components are either in LNGS, or ordered for delivery in October or November. The orders
include the external shielding, the crystal insertion system, and the crystal enclosure.
•
Provided there are no further delays, we expect to assemble the detector and begin commissioning by the end
of 2017.
PoP
Milestones
Schedule
M
i
l
e
s
t
o
n
e
s
c
o
m
p
l
e
t
i
o
n
D
a
t
e
1.
Veto vessel dry commissioning (
H
all B)
July 31
st
, 2017
2.
Hall C Site
available
(5 months after Hall C vacated)
May 1
2
th
3.
Lower Lead shielding
July 3rd
4.
PRA approval by LNGS
Sep 14th
5.
CIS delivery to LNGS
Sep 20th
6.
Crystal enclosure delivery to LNGS
Oct 15
th
7.
PE + SS +catch basin+ water tanks s
hielding delivery
to LNGS
Oct
15
th
8.
PE shielding installation in Hall C
Oct 31th
9.
Veto vessel cleaning +
Lumirror + PMTs
installation
in H
all C
Oct
31
th
10.
Electronics + DAQ installation in Hall C
Oct 31th
11.
Crystal insertion system installation inside the veto vessel
Nov 10th
12.
Fluid handling
installation in Hall C
Nov 30th
13.
5 kg c
rystal growt
h @ RMD
Oct
3nd
14.
Crystal enclosure delivery
to
PU
Oct
31
th
15.
Crystal-PMT installation in enclosure
in glove box @ PU
Nov 15
th
16.
Crystal shipment to LNGS
Nov 30
th
17.
Crystal installation in the vessel
Dec 10th
18.
LS preparation (to be done in advance, BX activity)
???
19.
Veto commissioning
End 2017
20.
PoP run
2018
Progress update on the SABRE crystal growth project, including setbacks, milestones, and expected completion dates. Recent advancements in crystal growing techniques and facility upgrades at Princeton University. Anticipated assembly and commissioning timeline at the end of 2017.
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Presentation Transcript
The SABRE Crystals Frank Calaprice
SABRE PoP NaI(Tl) Crystal Producer: Princeton University & RMD Company (Boston) Starting point: Astrograde powder by Sigma Aldrich with 9 ppb natK. 2kg test crystal In fall 2015 RMD grew a 2-kg crystal (3.5 diameter) with: 9 ppb natK (same as starting powder) < 0.1 ppb87Rb Measuredby ICP-MS: First crystal below DAMA ([K]~13 ppb, [Rb]<0.35 ppb) Research since then focused on: Growing full-scale 5-kg crystal ( 4 diameter) improving procedures for crystal growing to reduce background Powder drying, crucible purity, etc. Refined procedure for crystal handling (polishing, crystal mounting and handling inside the enclosure in glove box) Facilities at PU: new glove box installed inside Rn-free clean room Growth setbacks: Impurities in crystal-grade powder- now understood (?) RMD funded by DoE (1 M$) -> extra 50 kg of Astrograde powder 3 ppb in K Test growth of full-scale crystal with Astrograde Powder (AP) August 2017 1st crystal with RMD AP and crucible: Oct 3 2017 (still cooling ) 2nd crystal with PU AP and crucible: Nov. 2017 (starting soon) Glove box @ PU
SABRE PoP Summary Setbacks in crystal growth, delay of site preparation, and delay in purchase orders, all introduced several months of delay. We passed these problems and expect to good progress now. Growth of 1st 5-kg crystal is expected to finish in early October. A second will come in November. Fluid operations, blocked by laboratory management, can start under new agreement with Regional Authorities. With completed Safety Review, cleaning with fluids and scintillator operations should start soon. Most of the major components are either in LNGS, or ordered for delivery in October or November. The orders include the external shielding, the crystal insertion system, and the crystal enclosure. Provided there are no further delays, we expect to assemble the detector and begin commissioning by the end of 2017.
PoP Milestones Schedule Milestones Milestonescompletion completion Date Date 1. Veto vessel dry commissioning (Hall B) July 31st, 2017 2. Hall C Site available (5 months after Hall C vacated) May 12th 3. Lower Lead shielding July 3rd 4. PRA approval by LNGS Sep 14th 5. CIS delivery to LNGS Sep 20th 6. Crystal enclosure delivery to LNGS Oct 15th 7. PE + SS +catch basin+ water tanks shielding delivery to LNGS Oct 15th 8. PE shielding installation in Hall C Oct 31th 9. Veto vessel cleaning + Lumirror + PMTs installation in Hall C Oct 31th 10. Electronics + DAQ installation in Hall C Oct 31th 11. Crystal insertion system installation inside the veto vessel Nov 10th 12. Fluid handling installation in Hall C Nov 30th 13. 5 kg crystal growth @ RMD Oct 3nd 14. Crystal enclosure delivery to PU Oct 31th 15. Crystal-PMT installation in enclosure in glove box @ PU Nov 15th 16. Crystal shipment to LNGS Nov 30th 17. Crystal installation in the vessel Dec 10th 18. LS preparation (to be done in advance, BX activity) ??? 19. Veto commissioning End 2017 20. PoP 2018
