Lead Dust Sampling Technician - Laboratory Selection and Interpretation

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Selecting a Laboratory
and Interpreting Results
 
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Select an EPA-recognized lab
Maintain a chain of custody
Review and interpret lab results
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Submit samples to a lab recognized by EPA’s
National Lead Laboratory Accreditation
Program (NLLAP)
To locate a lab
Call the National Lead Information Center (NLIC) at
1-800-424-LEAD
Visit the EPA Web site at
www.epa.gov/lead/pubs/nllap.htm
See the fact sheet “Selecting a Lead
Laboratory” at the end of this chapter.
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Tell the lab you will be collecting dust wipe
samples for lead.
Ask:
Is the laboratory recognized to analyze for lead in
dust by NLLAP?
Will sampling materials be provided?
What is the turnaround time for analysis?
Can the laboratory analyze composite samples? (If
the client wants composite samples)
What is the cost per sample?
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Submit blank wipe samples.
Duplicate, or side by side sampling can
be used to check lab consistency.
Review all of your sample collection
and chain-of-custody forms.
Carefully review all lab results
.
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Confirm all information is recorded clearly
and correctly.
Sample numbers
Sample locations
Sample dimensions
Keep a copy for your records and note
blanks.
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A record of
 each person who handles the sample
from the time it is collected until it is sent to the lab.
The lead dust sampling technician is responsible
for maintaining chain of custody until he or she
transfers custody of the samples.
Include information on sampling form
A sample Chain of Custody form is shown on the
next page, and as an attachment to this chapter.
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Check for appropriate units (
g/ft
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Compare results to the EPA/HUD
clearance standards for lead dust:
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Answer the questions.
 
Be prepared to explain your answers.
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Mistaking 
weight
 (mass) for 
surface
loading
 by using incorrect units (
g for
g/ft
2
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Not submitting blank samples
Labeling or recording in the sample
log blank samples as blanks
Not maintaining a chain of custody
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Select an EPA-recognized lab.
Call 1-800-424-LEAD
Visit www.epa.gov/lead/pubs/nllap.htm
Ensure that the lab is EPA-recognized
for the analysis of lead in dust.
Maintain a chain of custody.
Interpret lab results.
Slide Note

Lead Dust Sampling Technician Training Course

4-

Chapter 4: Selecting a Laboratory and Interpreting Results

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Learn how to select a laboratory for lead dust sampling, maintain chain of custody, review and interpret lab results. Understand the importance of selecting an EPA-recognized lab, asking relevant questions, and ensuring quality control in the field. Detailed guidance on submitting samples, reviewing sample collection forms, and maintaining chain of custody is provided. Essential for Lead Dust Sampling Technicians.


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  1. 4-1 Chapter 4 Selecting a Laboratory and Interpreting Results Lead Dust Sampling Technician June 2013

  2. 4-2 Objectives Select an EPA-recognized lab Maintain a chain of custody Review and interpret lab results Lead Dust Sampling Technician June 2013

  3. 4-3 Selecting a Laboratory Submit samples to a lab recognized by EPA s National Lead Laboratory Accreditation Program (NLLAP) To locate a lab Call the National Lead Information Center (NLIC) at 1-800-424-LEAD Visit the EPA Web site at www.epa.gov/lead/pubs/nllap.htm See the fact sheet Selecting a Lead Laboratory at the end of this chapter. Lead Dust Sampling Technician June 2013

  4. 4-4 Questions To Ask Laboratories Tell the lab you will be collecting dust wipe samples for lead. Ask: Is the laboratory recognized to analyze for lead in dust by NLLAP? Will sampling materials be provided? What is the turnaround time for analysis? Can the laboratory analyze composite samples? (If the client wants composite samples) What is the cost per sample? Lead Dust Sampling Technician June 2013

  5. 4-5 Quality Control in the Field Submit blank wipe samples. Duplicate, or side by side sampling can be used to check lab consistency. Review all of your sample collection and chain-of-custody forms. Carefully review all lab results. Lead Dust Sampling Technician June 2013

  6. 4-6 Review Your Sample Collection Form Confirm all information is recorded clearly and correctly. Sample numbers Sample locations Sample dimensions Keep a copy for your records and note blanks. Lead Dust Sampling Technician June 2013

  7. 4-7 Chain of Custody A record of each person who handles the sample from the time it is collected until it is sent to the lab. The lead dust sampling technician is responsible for maintaining chain of custody until he or she transfers custody of the samples. Include information on sampling form A sample Chain of Custody form is shown on the next page, and as an attachment to this chapter. Lead Dust Sampling Technician June 2013

  8. 4-8 Lead Dust Sampling Technician June 2013

  9. 4-9 Evaluating Laboratory Results for Single Samples Check for appropriate units ( g/ft2) Compare results to the EPA/HUD clearance standards for lead dust: Floors < 40 g/ft2 passes Sills < 250 g/ft2 passes Troughs < 400 g/ft2 passes Lead Dust Sampling Technician June 2013

  10. 4-10 Activity: Interpreting Laboratory Results Turn to Attachment 4-D Answer the questions. Be prepared to explain your answers. Lead Dust Sampling Technician June 2013

  11. 4-11 Evaluating Laboratory Results for Composite Samples Location 2 Subsamples 3 Subsamples 4 Subsamples Floors 40 g/ft2 27 g/ft2 20 g/ft2 Sills 250 g/ft2 167 g/ft2 125 g/ft2 Troughs 400 g/ft2 267 g/ft2 200 g/ft2 Lead Dust Sampling Technician June 2013

  12. 4-12 Avoiding Common Mistakes Mistaking weight (mass) for surface loading by using incorrect units ( g for g/ft2) Not submitting blank samples Labeling or recording in the sample log blank samples as blanks Not maintaining a chain of custody Lead Dust Sampling Technician June 2013

  13. 4-13 Summary Select an EPA-recognized lab. Call 1-800-424-LEAD Visit www.epa.gov/lead/pubs/nllap.htm Ensure that the lab is EPA-recognized for the analysis of lead in dust. Maintain a chain of custody. Interpret lab results. Lead Dust Sampling Technician June 2013

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