State Crime Lab Drug Sampling Protocols

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Using the State Crime Lab’s
Drug Sampling Protocols for
the Defense
 
By Andrew DeSimone
Assistant Appellate Defender
 
The Current Law
 
“‘When a random sample from a quantity
of tablets or capsules identical in
appearance is analyzed and is found to
contain contraband, the entire quantity may
be introduced as the contraband.’”  
State v.
Myers
, 61 N.C. App. 554, 556, 301 S.E.2d
401, 407 (1983) (citation omitted).
 
Three Sampling Methods
 
1. Administrative Sample
Selection
2. Threshold Sample Selection
3. Hypergeometric Sampling
Plan
 
THE HYPERGEOMETRIC SAMPLING
PLAN IS THE ONLY METHOD THAT
ALLOWS THE EXPERT TO REPORT ANY
ASSUMPTIONS ABOUT THE CHEMICAL
COMPOSITION OF THE 
UNANALYZED
UNITS.
 
If the analyst offers an opinion about the
composition of the unanalyzed material (except
when using the hypergeometric plan), object
under…
 
1. Rule 702
2. Rule 401
3. Rule 602
4. Federal and State Due Process Grounds
 
Pretrial Preparation
 
1. Determine what sampling method the analyst
used
2. Figure out, and make sure you have, the
protocol that was in effect at the time of the
testing.
3. Consider meeting with the analyst before trial.
4. Consider talking with your own expert.
5. File a motion 
in limine 
or request 
voir dire 
of
the expert at trial.
 
Administrative Sample Selection
 
“A practice for pharmaceutical preparations and for
items when a statutory threshold does not apply.”
The analyst does a complete chemical analysis of
one unit.  The analyst can only report the chemical
composition of the single analyzed pill.
As for the rest, the most the analyst can say is:
“‘The physical characteristics, including shape,
color and manufacturer’s markings of all units were
visually examined and found to be consistent with a
pharmaceutical preparation containing (insert
substance(s) indicated).”
 
Sample Lab Report
 
Make the Distinction:
 
 
“analyzed and found to contain”
“visually examined and found to
be consistent with”
 
Comparing Two Versions of the Administrative
Sample Selection Protocol
 
Version 8: Effective August 29, 2014
3.0 Definitions
Administrative Sample Selection
 - A practice for
pharmaceutical preparations and for items when a
statutory threshold does not apply. 
No inferences about
unanalyzed material are made.
 
Version 10: Effective October 19, 2015
3.0 Definitions
Administrative Sample Selection
 - A practice for
pharmaceutical preparations and for items when a
statutory threshold does not apply. 
No inferences about
unanalyzed 
non-pharmaceutical 
material are made.
 
If the analyst gives an opinion on the chemical
composition of the whole population…
 
1. Raise a discovery violation
2. Object to the opinion under Rules 401,
602, 702, and on federal and state due
process grounds
3. Impeach the analyst
 
N.C. Gen. Stat. § 15A-903(a)(2)
 
Upon motion of the defendant, the court must order:
 
The prosecuting attorney to give notice to the defendant
of any expert witnesses that the State reasonably expects
to call as a witness at trial. Each such witness shall
prepare, and 
the State shall furnish to the defendant, a
report of the results of any examinations or tests
conducted by the expert. 
The State shall also furnish to
the defendant the expert's curriculum vitae, 
the
expert's opinion
, and the underlying basis for that
opinion.
 The State shall give the notice and furnish the
materials required by this subsection within a reasonable
time prior to trial, as specified by the court....
 
N.C. Gen. Stat. §15A-910(a)
 
If at any time during the course of the proceedings the
court determines that a party has failed to comply with
this Article or with an order issued pursuant to this
Article, the court in addition to exercising its contempt
powers may
(1)  Order the party to permit the discovery or
inspection, or
(2)  Grant a continuance or recess, or  
[to consult
with/obtain your own expert]
(3)  Prohibit the party from introducing evidence not
disclosed
, 
[preferable] 
or
(3a)  Declare a mistrial, or
(3b)  Dismiss the charge, with or without prejudice, or
(4)  Enter other appropriate orders
 
Object under . . .
 
1. Rule 702
2. Rule 401
3. Rule 602
4. Federal and State Due Process
Grounds
 
 
State Crime Lab’s Administrative Procedure
for Sampling
 
5.0 References
Guidelines on Representative Drug Sampling
. United
Nations, New York: United Nations Office on Drugs and
Crime, 2009.
Frank, Richard S., et. al. "Representative Sampling of Drug
Seizures in Multiple Containers." 
Journal of Forensic
Sciences, 
Volume 36, Issue 2 (March 1991), 350-357.
“PART III A - Methods of Analysis/Sampling Seized Drugs
for Qualitative Analysis.” 
Scientific Working Group for the
Analysis of Seized Drugs (SWGDRUG) Recommendations.
5th ed.: January 29, 2010.
 
SWGDRUG Standards:
 
2.1.1.2: “If an inference about the whole population is to be
drawn from a sample, then the plan shall be statistically
based and limits of the inference shall be documented.”
3.2.2.1: “Statistical approaches are applicable when
inferences are made about the whole population.”
3.2.2.2: “Non-statistical approaches are appropriate if no
inference is to be made about the whole population.”
4: “SWGDRUG recommends that each unit comprising the
sample shall be analyzed to meet the SWGDRUG minimum
recommendations (Part IIIB) for forensic drug identification,
if statistical inferences are to be made about the whole
population.”
5: “Inferences drawn from the application of the sampling
plan and subsequent analyses shall be documented.”
 
ASTM Standards:
 
4.2.1.2: “If an inference about the whole population is to
be drawn from a sample, then the plan should be
statistically based and limits of the inference shall be
documented.”
 4.2.2: “Statistically selected units shall be analyzed to
meet Practice E2329 if statistical inferences are to be made
about the whole population.”
5.5.1: “Statistical approaches are applicable when
inferences are made about the whole population.”
5.5.2: “Non-statistical approaches are appropriate if no
inference is to be made about the whole population.”
 7.1: “Inferences based on use of a sampling plan and
concomitant analysis shall be documented.”
 
Impeach the analyst
 
Use the protocol, the lab report, and the SWGDRUG
and ASTM Standards
Elicit Evidence that the analyst did not apply the
threshold or hypergeometric sampling plans
Elicit evidence that the protocol provides: “If additional
testing is needed, the prosecuting attorney in the case
may contact the Forensic Scientist Manager of the Drug
Chemistry Section.”  Thus, the State had the means to
test the material in a manner that might have permitted
inferences about the chemical content of whole
population, but did not pursue those options
 
If the analyst conforms his/her testimony to
the protocol and only gives an opinion as to
the contents of the analyzed portion (which
does not satisfy the weight threshold) move
to dismiss for insufficient evidence on that
particular ground.
Request an instruction on a lesser-included
offense.
Use the analyst’s testimony and/or the
protocol in closing argument.
 
Threshold Sample Selection
 
The analyst does a chemical analysis of
a sufficient number of units “to satisfy
the statutory threshold[.]”
 
Hypergeometric Sampling Plan
 
The analyst does a complete chemical analysis of
the number of packages in a table provided in the
protocol relative to the size of the entire population.
The analyst then extrapolates the weight of the
entire population.
The analyst must report:
“‘This material was analyzed with a statistical
sampling plan that demonstrates with 95% confidence
that at least 90% of the material contains the identified
substance(s).’”
 
Hypergeometric Sampling Plan Table
 
State v. James
, 770 S.E.2d 736 (2015)
 
The defendant was convicted of trafficking in 28 grams or
more of opium by possession and transportation, and
PWISD opium, all for 65 oxycodone pills.
The analyst stuck to the Administrative Sample Selection
protocol and only gave her opinion that the two pills tested,
weighing .99 grams, contained oxycodone.
The Court of Appeals held:
“Defendant did not cross-examine Agent Matkowsky regarding
the sufficiency of the sample size and did not make the
sufficiency of the sample size a basis for his motion to
dismiss.”  Therefore, the Court of Appeals dismissed the
argument that the State presented insufficient evidence and
refused to take judicial notice of the protocol.
 
Dicta
 in 
State v. James
 
“Agent Matkowsky testified that she visually
inspected the remaining untested pills and
concluded that with regard to color, shape, and
imprint, they were ‘consistent with’ those pills that
tested positive for oxycodone.  The total weight of
the pills was 31.79 grams, exceeding the 28 gram
requirement for trafficking.  As a result, the State
presented sufficient evidence to conclude that
defendant possessed and transported 28 grams or
more of a Schedule II controlled substance.”
 
State v. Lewis
, 779 S.E.2d 147 (2015)
 
The defendant was convicted of, 
inter alia
, conspiracy to traffic
14 grams or more but less than 28 grams of opiates for 20 pills
 The analyst stuck to the Administrative Sample Selection
protocol and only gave an opinion that the one pill that was tested
tested, weighing .88 grams, contained oxycodone.
The Court of Appeals held the trial court did not err by failing to
instruct the jury on the requested lesser-included conspiracy to
traffic offenses
 
Get Your Own Expert . . .
 
To testify that there can be no reliable
determination of the chemical composition
of an entire population of pills based upon a
non-statistical approach like administrative
sample selection.
 
State v. Riera
, 276 N.C. 361, 172 S.E.2d 535 (1970)
 
The defendant was charged with possession of a barbiturate drug
for the purpose of sale, barter, exchange, etc., a felony.  The statute
at issue provided that “possession of one hundred or more tablets,
capsules or other dosage forms… shall be prima facie evidence” of
the felony.   An expert randomly selected and chemically tested
“some” of the 205 capsules the defendant possessed and found
those capsules to contain two distinct barbiturates that were
constituent parts of a drug sold under the name “Tuinal.”  The
expert also testified “the remaining capsules were all identical in
coloration, each had an identical code number – ‘Lilly F 65’ –
impressed upon it, and the code number indicated that it contained
Tuinal.”
Although the Court rejected the sufficiency argument, the Court
granted a new trial because the trial court erred by failing to instruct
on the lesser included offense of misdemeanor simple possession of
a barbiturate drug, as there was “ample evidence” to support it.
 
Other Trial Considerations
 
1. Request Complete Recordation
2. Make the protocol and the SWGDRUG
and ASTM Standards part of the record
3. Continue to object to preserve the
issue(s) for appeal
 
4. Ask for a modification to the pattern
instruction on expert testimony.
5. Constitutionalize all objections.
 
Contact the Office of the Appellate
Defender for a Consult
 
Feel free to contact us at any time.  We
always have two lawyers on call to consult
with attorneys across the state.
 
  
Office of the Appellate Defender
  
123 W. Main Street, Suite 500
  
Durham, North Carolina 27701
  
(919) 354-7210
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Using the State Crime Lab's drug sampling protocols for defense involves understanding three sampling methods: administrative sample selection, threshold sample selection, and hypergeometric sampling plan. The hypergeometric plan allows experts to make assumptions about the chemical composition of unanalyzed units. If an analyst offers an opinion about unanalyzed materials without using the hypergeometric plan, they must meet certain rules. Pretrial preparation is crucial, including determining the sampling method used, obtaining the testing protocol, and engaging with expert witnesses.

  • Crime Lab
  • Drug Sampling
  • Defense
  • Sampling Methods
  • Expert Witness

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  1. Using the State Crime Labs Drug Sampling Protocols for the Defense By Andrew DeSimone Assistant Appellate Defender

  2. https://encrypted-tbn1.gstatic.com/images?q=tbn:ANd9GcReX97-a5SkXkQuJvmdl1cYinR2HX4fM1CCxyxC3ZiSDjSAf43H4Ahttps://encrypted-tbn1.gstatic.com/images?q=tbn:ANd9GcReX97-a5SkXkQuJvmdl1cYinR2HX4fM1CCxyxC3ZiSDjSAf43H4A

  3. The Current Law When a random sample from a quantity of tablets or capsules appearance is analyzed and is found to contain contraband, the entire quantity may be introduced as the contraband. State v. Myers, 61 N.C. App. 554, 556, 301 S.E.2d 401, 407 (1983) (citation omitted). identical in

  4. Three Sampling Methods 1. Administrative Sample Selection 2. Threshold Sample Selection 3. Hypergeometric Sampling Plan

  5. THE PLAN IS THE ONLY METHOD THAT ALLOWS THE EXPERT TO REPORT ANY ASSUMPTIONS ABOUT THE CHEMICAL COMPOSITION OF THE UNANALYZED UNITS. HYPERGEOMETRIC SAMPLING

  6. If the analyst offers an opinion about the composition of the unanalyzed material (except when using the hypergeometric plan), object under 1. Rule 702 2. Rule 401 3. Rule 602 4. Federal and State Due Process Grounds

  7. Pretrial Preparation 1. Determine what sampling method the analyst used 2. Figure out, and make sure you have, the protocol that was in effect at the time of the testing. 3. Consider meeting with the analyst before trial. 4. Consider talking with your own expert. 5. File a motion in limine or request voir dire of the expert at trial.

  8. Administrative Sample Selection A practice for pharmaceutical preparations and for items when a statutory threshold does not apply. The analyst does a complete chemical analysis of one unit. The analyst can only report the chemical composition of the single analyzed pill. As for the rest, the most the analyst can say is: The physical characteristics, including shape, color and manufacturer s markings of all units were visually examined and found to be consistent with a pharmaceutical preparation containing (insert substance(s) indicated).

  9. Sample Lab Report

  10. Make the Distinction: analyzed and found to contain visually examined and found to be consistent with

  11. Comparing Two Versions of the Administrative Sample Selection Protocol Version 8: Effective August 29, 2014 3.0 Definitions Administrative Sample Selection -A practice for pharmaceutical preparations and for items when a statutory threshold does not apply. No inferences about unanalyzed material are made. Version 10: Effective October 19, 2015 3.0 Definitions Administrative Sample Selection -A practice for pharmaceutical preparations and for items when a statutory threshold does not apply. No inferences about unanalyzed non-pharmaceutical material are made.

  12. If the analyst gives an opinion on the chemical composition of the whole population 1. Raise a discovery violation 2. Object to the opinion under Rules 401, 602, 702, and on federal and state due process grounds 3. Impeach the analyst

  13. N.C. Gen. Stat. 15A-903(a)(2) Upon motion of the defendant, the court must order: The prosecuting attorney to give notice to the defendant of any expert witnesses that the State reasonably expects to call as a witness at trial. Each such witness shall prepare, and the State shall furnish to the defendant, a report of the results of any examinations or tests conducted by the expert. The State shall also furnish to the defendant the expert's curriculum vitae, the expert's opinion, and the underlying basis for that opinion. The State shall give the notice and furnish the materials required by this subsection within a reasonable time prior to trial, as specified by the court....

  14. N.C. Gen. Stat. 15A-910(a) If at any time during the course of the proceedings the court determines that a party has failed to comply with this Article or with an order issued pursuant to this Article, the court in addition to exercising its contempt powers may (1) Order the party to permit the discovery or inspection, or (2) Grant a continuance or recess, or [to consult with/obtain your own expert] (3) Prohibit the party from introducing evidence not disclosed, [preferable] or (3a) Declare a mistrial, or (3b) Dismiss the charge, with or without prejudice, or (4) Enter other appropriate orders

  15. Object under . . . 1. Rule 702 2. Rule 401 3. Rule 602 4. Federal and State Due Process Grounds

  16. State Crime Labs Administrative Procedure for Sampling 5.0 References Guidelines on Representative Drug Sampling. United Nations, New York: United Nations Office on Drugs and Crime, 2009. Frank, Richard S., et. al. "Representative Sampling of Drug Seizures in Multiple Containers." Journal of Forensic Sciences, Volume 36, Issue 2 (March 1991), 350-357. PART III A - Methods of Analysis/Sampling Seized Drugs for Qualitative Analysis. Scientific Working Group for the Analysis of Seized Drugs (SWGDRUG) Recommendations. 5th ed.: January 29, 2010.

  17. SWGDRUG Standards: 2.1.1.2: If an inference about the whole population is to be drawn from a sample, then the plan shall be statistically based and limits of the inference shall be documented. 3.2.2.1: Statistical approaches are applicable when inferences are made about the whole population. 3.2.2.2: Non-statistical approaches are appropriate if no inference is to be made about the whole population. 4: SWGDRUG recommends that each unit comprising the sample shall be analyzed to meet the SWGDRUG minimum recommendations (Part IIIB) for forensic drug identification, if statistical inferences are to be made about the whole population. 5: Inferences drawn from the application of the sampling plan and subsequent analyses shall be documented.

  18. ASTM Standards: 4.2.1.2: If an inference about the whole population is to be drawn from a sample, then the plan should be statistically based and limits of the inference shall be documented. 4.2.2: Statistically selected units shall be analyzed to meet Practice E2329 if statistical inferences are to be made about the whole population. 5.5.1: Statistical approaches are applicable when inferences are made about the whole population. 5.5.2: Non-statistical approaches are appropriate if no inference is to be made about the whole population. 7.1: Inferences based on use of a sampling plan and concomitant analysis shall be documented.

  19. Impeach the analyst Use the protocol, the lab report, and the SWGDRUG and ASTM Standards Elicit Evidence that the analyst did not apply the threshold or hypergeometric sampling plans Elicit evidence that the protocol provides: If additional testing is needed, the prosecuting attorney in the case may contact the Forensic Scientist Manager of the Drug Chemistry Section. Thus, the State had the means to test the material in a manner that might have permitted inferences about the chemical content of whole population, but did not pursue those options

  20. If the analyst conforms his/her testimony to the protocol and only gives an opinion as to the contents of the analyzed portion (which does not satisfy the weight threshold) move to dismiss for insufficient evidence on that particular ground. Request an instruction on a lesser-included offense. Use the analyst s testimony and/or the protocol in closing argument.

  21. Threshold Sample Selection The analyst does a chemical analysis of a sufficient number of units to satisfy the statutory threshold[.]

  22. Hypergeometric Sampling Plan The analyst does a complete chemical analysis of the number of packages in a table provided in the protocol relative to the size of the entire population. The analyst then extrapolates the weight of the entire population. The analyst must report: This material was analyzed with a statistical sampling plan that demonstrates with 95% confidence that at least 90% of the material contains the identified substance(s).

  23. Hypergeometric Sampling Plan Table

  24. State v. James, 770 S.E.2d 736 (2015) The defendant was convicted of trafficking in 28 grams or more of opium by possession and transportation, and PWISD opium, all for 65 oxycodone pills. The analyst stuck to the Administrative Sample Selection protocol and only gave her opinion that the two pills tested, weighing .99 grams, contained oxycodone. The Court ofAppeals held: Defendant did not cross-examine Agent Matkowsky regarding the sufficiency of the sample size and did not make the sufficiency of the sample size a basis for his motion to dismiss. Therefore, the Court of Appeals dismissed the argument that the State presented insufficient evidence and refused to take judicial notice of the protocol.

  25. Dicta in State v. James Agent Matkowsky testified that she visually inspected the remaining concluded that with regard to color, shape, and imprint, they were consistent with those pills that tested positive for oxycodone. The total weight of the pills was 31.79 grams, exceeding the 28 gram requirement for trafficking. As a result, the State presented sufficient evidence to conclude that defendant possessed and transported 28 grams or more of a Schedule II controlled substance. untested pills and

  26. State v. Lewis, 779 S.E.2d 147 (2015) The defendant was convicted of, inter alia, conspiracy to traffic 14 grams or more but less than 28 grams of opiates for 20 pills The analyst stuck to the Administrative Sample Selection protocol and only gave an opinion that the one pill that was tested tested, weighing .88 grams, contained oxycodone. The Court of Appeals held the trial court did not err by failing to instruct the jury on the requested lesser-included conspiracy to traffic offenses

  27. Get Your Own Expert . . . To testify that there can be no reliable determination of the chemical composition of an entire population of pills based upon a non-statistical approach like administrative sample selection.

  28. State v. Riera, 276 N.C. 361, 172 S.E.2d 535 (1970) The defendant was charged with possession of a barbiturate drug for the purpose of sale, barter, exchange, etc., a felony. The statute at issue provided that possession of one hundred or more tablets, capsules or other dosage forms shall be prima facie evidence of the felony. An expert randomly selected and chemically tested some of the 205 capsules the defendant possessed and found those capsules to contain two distinct barbiturates that were constituent parts of a drug sold under the name Tuinal. The expert also testified the remaining capsules were all identical in coloration, each had an identical code number Lilly F 65 impressed upon it, and the code number indicated that it contained Tuinal. Although the Court rejected the sufficiency argument, the Court granted a new trial because the trial court erred by failing to instruct on the lesser included offense of misdemeanor simple possession of a barbiturate drug, as there was ample evidence to support it.

  29. Other Trial Considerations 1. Request Complete Recordation 2. Make the protocol and the SWGDRUG and ASTM Standards part of the record 3. Continue to object to preserve the issue(s) for appeal constant vigilance 4. Ask for a modification to the pattern instruction on expert testimony. 5. Constitutionalize all objections.

  30. Contact the Office of the Appellate Defender for a Consult Feel free to contact us at any time. always have two lawyers on call to consult with attorneys across the state. We Office of theAppellate Defender 123 W. Main Street, Suite 500 Durham, North Carolina 27701 (919) 354-7210

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